InfraLensInfraLens
IS CodesIRCToolsSORHandbookQA/QCPMCFormatsCPHEEOMapsProjectsDCRRulesAbout Join Channel
Join
IS CodesIRCToolsSORHandbookQA/QCPMCFormatsCPHEEOMapsProjectsDCRDesign RulesBIMAbout Join WhatsApp Channel
InfraLensInfraLens
IS CodesIRCToolsSORHandbookQA/QCPMCFormatsCPHEEOMapsProjectsDCRRulesAbout Join Channel
Join
IS CodesIRCToolsSORHandbookQA/QCPMCFormatsCPHEEOMapsProjectsDCRDesign RulesBIMAbout Join WhatsApp Channel

IS 5282 : 1969Liquid sedimentation methods for determination of particle size of powders

PDFGoogleCompareBIS Portal
Link points to Internet Archive / others. Not hosted by InfraLens. Details
ISO 13317-2
CurrentSpecializedTesting MethodMaterials Science · Sieves, Sieving and Other Sizing Methods
PDFGoogleCompareBIS Portal
Link points to Internet Archive / others. Not hosted by InfraLens. Details
OverviewValues3InternationalTablesFAQ3Related

IS 5282:1969 is the Indian Standard (BIS) for liquid sedimentation methods for determination of particle size of powders. This standard prescribes liquid sedimentation methods for determining the particle size distribution of fine powders in the sub-sieve range. It covers procedures such as the pipette method and the sedimentation balance method, which utilize Stokes' Law to calculate particle size based on settling velocity in a viscous fluid.

Liquid sedimentation methods for determination of particle size of powders

Overview

Status
Current
Usage level
Specialized
Domain
Materials Science — Sieves, Sieving and Other Sizing Methods
Type
Testing Method
International equivalents
ISO 13317-2:2007 · International Organization for Standardization, Switzerland
Typically used with
IS 460IS 4879IS 5258
Also on InfraLens for IS 5282
3Key values3FAQs
Practical Notes
! Proper and complete dispersion of the powder in the liquid is critical; failure to break up agglomerates will artificially increase the apparent particle size.
! Strict temperature control (usually via a water bath) is necessary because the viscosity of the suspending liquid changes significantly with temperature, directly affecting sedimentation velocity.
! The test calculates an 'equivalent spherical diameter'. For highly irregular, flaky, or needle-like particles, results may differ from actual physical dimensions obtained via microscopy.
Frequently referenced clauses
Cl. 3Principle of SedimentationCl. 4Pipette Method (Andreasen Method)Cl. 5Sedimentation Balance MethodCl. 6Preparation of Suspensions and DispersionCl. 7Evaluation of Results
Pulled from IS 5282:1969. Browse the full clause & table index below in Tables & Referenced Sections.
powdersfine particlessuspensionssoilspigmentscement

International Equivalents

Similar International Standards
BS 3406-2:1963British Standards Institution, UK
HighWithdrawn
Methods for the determination of particle size of powders. Liquid sedimentation methods
This standard is a direct historical equivalent, covering liquid sedimentation methods for particle size determination of powders.
ISO 13317-2:2007International Organization for Standardization, Switzerland
HighCurrent
Particle size analysis — Determination of particle size distribution by gravitational sedimentation methods — Part 2: Fixed pipet method
Specifies the fixed pipet method, a key liquid sedimentation technique likely covered by IS 5282, for determining particle size distribution.
ASTM D422-63 (Reapproved 2007)ASTM International, USA
MediumWithdrawn
Standard Test Method for Particle-Size Analysis of Soils (Hydrometer Method)
Outlines the hydrometer method, another fundamental liquid sedimentation technique, applicable to fine particles despite its primary focus on soils.
Key Differences
≠IS 5282:1969, being an older standard, typically provides less prescriptive guidance on modern instrumental aspects, automated data acquisition, and advanced dispersion techniques compared to contemporary international standards.
≠Modern international standards like ISO 13317-2 often specify tighter temperature control tolerances (e.g., ±0.1°C to ±0.5°C) and more detailed requirements for temperature monitoring during the test than older standards.
≠Reporting of results in IS 5282:1969 may be less aligned with modern data processing and graphical representation standards (e.g., ISO 9276 series) which provide more comprehensive guidelines for statistical analysis and presentation of particle size distributions.
≠While IS 5282 covers 'powders', ASTM D422 is specifically for 'soils', leading to differences in sample preparation details and considerations for organic matter or specific soil mineralogy.
≠Modern standards often include detailed uncertainty analysis and quality control procedures, which are generally less elaborated upon in older standards like IS 5282:1969.
Key Similarities
≈All standards are fundamentally based on Stokes' Law, which describes the settling velocity of spherical particles in a viscous fluid under gravity, allowing for the calculation of particle diameter.
≈They all utilize liquid sedimentation methods, primarily the pipette method and/or the hydrometer method, to determine the particle size distribution of fine powders or soil particles.
≈Common to all is the requirement for effective dispersion of the sample in a liquid medium (typically water) using a suitable dispersing agent to prevent flocculation and ensure individual particle settling.
≈Each standard emphasizes the importance of maintaining a controlled temperature for the sedimentation suspension and applying corrections for changes in liquid viscosity due to temperature variations.
≈All standards aim to determine the cumulative percentage by mass of particles finer than a given diameter at various time intervals, leading to a particle size distribution curve.
Parameter Comparison
ParameterIS ValueInternationalSource
Lower limit of particle size rangeApproximately 1 µmApproximately 1 µmBS 3406-2:1963 and ASTM D422-63
Upper limit of particle size rangeApproximately 75 µm (passing No. 200 sieve)Approximately 75 µm (passing No. 200 sieve)BS 3406-2:1963 and ASTM D422-63
Nominal test temperatureControlled temperature (e.g., 20°C to 30°C)20°C (or 23°C)BS 3406-2:1963 and ISO 13317-2:2007
Test temperature toleranceControlled (specific tolerance not explicitly detailed in publicly available summaries for 1969 standard, likely ±0.5 to ±1°C)±0.5°C to ±1°C (ISO 13317-2 allows tighter control of ±0.1°C to ±0.5°C)BS 3406-2:1963 and ASTM D422-63 (ISO 13317-2 for modern standard)
Primary dispersing agentSodium hexametaphosphate (e.g., Calgon)Sodium hexametaphosphateBS 3406-2:1963, ISO 13317-2:2007, and ASTM D422-63
Method for calculating particle diameterStokes' LawStokes' LawAll listed international standards
⚠ Verify details from original standards before use

Key Values3

Quick Reference Values
Typical particle size range1 to 75 micrometers
Maximum Reynolds number for Stokes' law validity0.2
Recommended suspension concentration0.2% to 2.0% by volume
Key Formulas
D = sqrt((18 * η * v) / (g * (ρ_s - ρ_l))) — Stokes' Law for calculating the equivalent spherical diameter of a settling particle

Tables & Referenced Sections

Key Tables
No tables data
Key Clauses
Clause 3 - Principle of Sedimentation
Clause 4 - Pipette Method (Andreasen Method)
Clause 5 - Sedimentation Balance Method
Clause 6 - Preparation of Suspensions and Dispersion
Clause 7 - Evaluation of Results

Related Resources on InfraLens

Cross-Referenced Codes
IS 460:2000Test Sieves: Part-I Wire Cloth Test Sieves
→
IS 4879:1968Method of sub-division of a gross sample of p...
→
IS 5258:1969Determination of particle size of powders by ...
→

Frequently Asked Questions3

What is the primary physical law governing this test method?+
Stokes' Law, which relates the terminal settling velocity of a spherical particle to its diameter, fluid viscosity, and density difference.
What is the effective particle size range for sedimentation methods?+
It is most effective for particles between 1 and 75 microns. Particles larger than this may fall too fast (causing turbulent flow), and smaller particles are affected by Brownian motion.
Why must the concentration of the suspension be kept low?+
To ensure free settling conditions. High concentrations lead to hindered settling, where particles interact and fall at rates not predicted by Stokes' Law.

QA/QC Inspection Templates

📋
QA/QC templates coming soon for this code.
Browse all 300 templates →